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how to use excel
®
in analytical chemistry
and in general scientific data analysis
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how to use
excel
®
in analytical
chemistry
and in general scientific
data analysis
Robert de Levie
Bowdoin College,Brunswick,ME
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         
The Pitt Building, Trumpington Street, Cambridge, United Kingdom
  
The Edinburgh Building, Cambridge CB2 2RU, UK
40 West 20th Street, New York, NY 10011-4211, USA
477 Williamstown Road, Port Melbourne, VIC 3207, Australia
Ruiz de Alarcón 13, 28014 Madrid, Spain
Dock House, The Waterfront, Cape Town 8001, South Africa
http://www.cambridge.org
First published in printed format 
ISBN 0-521-64282-5 hardback
ISBN 0-521-64484-4 paperback
ck
ISBN 0-511-04037-7 eBook
R. de Levie 2004
2001
(netLibrary)
©
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contents
Preface [xi]
part i introduction to using the spreadsheet
1 How to use Excel
[1]
1.1 Starting Windows [2]
1.2 A first look at the spreadsheet [3]
1.3 A simple spreadsheet and graph [7]
1.3a  Making a graph in Excel 97 or a more recent version [9]
1.3b Making a graph in Excel 5 or Excel 95 [11]
1.4 Addressing a spreadsheet cell [13]
1.5 More on graphs [15]
1.6 Mathematical operations [21]
1.7 Error messages [26]
1.8 Naming and annotating cells [27]
1.9 Viewing the spreadsheet [28]
1.10 Printing [29]
1.11 Help! [30]
1.12 The case of the changing options [31]
1.13 Importing macros and data [32]
1.14 Differences between the various versions of Excel [33]
1.15 Some often-used spreadsheet commands [35]
1.16 Changing the default settings [36]
1.17 Summary [37]
part ii statistics and related methods
2 Introduction to statistics
[39]
2.1 Gaussian statistics [39]
2.2 Replicate measurements [45]
v
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2.3 The propagation of imprecision from a single parameter [51]
2.4 The propagation of imprecision from multiple parameters [54]
2.5 The weighted average [58]
2.6 Least-squares fitting to a proportionality [60]
2.7 Least-squares fitting to a general straight line [66]
2.8 Looking at the data [71]
2.9 What is ‘normal’? [73]
2.10 Poissonian statistics [78]
2.11 How likely is the improbable? [79]
2.12 Summary [83]
3 More on least squares
[90]
3.1 Multi-parameter fitting [90]
3.2 Fitting data to a quadratic [93]
3.3 Least squares for equidistant data: smoothing and di fferentiation [94]
3.4 Weighted least squares [99]
3.5 Another example of weighted least squares: enzyme kinetics [103]
3.6 Non-linear data fitting [105]
3.6a  Some kinetic data [106]
3.6b A double exponential [109]
3.6c  False minima [115]
3.6d Enzyme kinetics revisited [116]
3.6e  SolverAid [117]
3.7 Summary [118]
part iii chemical equilibrium
4 Acids, bases, and salts
[121]
4.1 The mass action law and its graphical representations [121]
4.2 Conservation laws, proton balance, and pH calculations [127]
4.3 Titrations of monoprotic acids and bases [130]
4.4 Schwartz and Gran plots [133]
4.5 The first derivative [136]
4.6 A more general approach to data fitting [142]
4.7 Buffer action [146]
4.8 Diprotic acids and bases, and their salts [148]
4.9 Polyprotic acids and bases, and their salts [152]
4.10 Activity corrections [155]
4.11 A practical example [161]
4.12 Summary [172]
5 Other ionic equilibria
[175]
5.1 Complex formation [175]
vi
Contents
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5.2 Chelation [180]
5.3 Extraction [182]
5.4 Solubility [185]
5.5 Precipitation and dissolution [190]
5.6 Precipitation titrations [194]
5.7 The von Liebig titration [200]
5.8 The graphical representation of electrochemical equilibria [204]
5.9 Redox titrations [211]
5.10 Redox buffer action [217]
5.11 Summary [220]
part iv instrumental methods
6 Spectrometry, chromatography, and voltammetry
[223]
6.1 Spectrometric pK
a
determination [223]
6.2 Multi-component spectrometric analysis 1 [225]
6.3 Multi-component spectrometric analysis 2 [227]
6.4 The absorbance–absorbance diagram [231]
6.5 Chromatographic plate theory 1 [234]
6.6 Chromatographic plate theory 2 [239]
6.7 Peak area, position, and width [243]
6.8 Determining the number of theoretical plates [245]
6.9 Optimizing the mobile phase velocity [248]
6.10 Polarography [251]
6.11 Linear sweep and cyclic voltammetry 1 [257]
6.12 Linear sweep and cyclic voltammetry 2 [261]
6.13 Summary [263]
part v mathematical methods
7 Fourier transformation
[265]
7.1 Introduction to Fourier transformation [265]
7.2 Interpolation and filtering [277]
7.3 Differentiation [285]
7.4 Aliasing and leakage [288]
7.5 Convolution [295]
7.6 Deconvolution [304]
7.7 Summary [309]
8 Standard mathematical operations
[311]
8.1 The Newton–Raphson method [311]
8.2 Non-linear least squares [313]
8.3 Signal averaging [314]
Contents
vii
8.4 Lock-in amplification [316]
8.5 Data smoothing [318]
8.6 Peak fitting [324]
8.7 Integration [328]
8.8 Differentiation [331]
8.9 Semi-integration and semi-di fferentiation [335]
8.10 Interpolation [336]
8.11 Matrix manipulation [337]
8.12 Overflow [341]
8.13 Summary [343]
9 Numerical simulation of chemical kinetics
[345]
9.1 Introduction [345]
9.2 The explicit method [346]
9.2a  First-order kinetics [346]
9.2b Numerical accuracy [348]
9.2c  Dimerization kinetics [350]
9.2d A user-defined function to make the spreadsheet more e fficient [351]
9.2e  Trimerization kinetics [353]
9.2f  Monomer–dimer kinetics [354]
9.2g  Polymerization kinetics [355]
9.3 Implicit numerical simulation [359]
9.3a  First-order kinetics [359]
9.3b Dimerization kinetics [360]
9.3c  Trimerization kinetics [361]
9.3d Monomer–dimer kinetics [362]
9.3e  Polymerization kinetics [363]
9.4 Some applications [365]
9.4a  Autocatalysis [365]
9.4b Heterogeneous catalysis [367]
9.4c  The steady-state approximation [369]
9.4d Oscillating reactions: the Lotka model [372]
9.5 Summary [374]
part vi spreadsheet programming
10 Some useful macros
[375]
10.1 What is a macro? [375]
10.1a The macro module [376]
10.1b Reading and modifying the contents of a single cell [378]
10.1c  Reading and modifying the contents of a block of cells [382]
10.1d Two different approaches to modifying a block of cells [384]
10.1e  Numerical precision [387]
viii
Contents
10.1f  Communication via boxes [389]
10.1g  Subroutines [393]
10.2 A case study: interpolating in a set of equidistant data [395]
10.2a  Step-by-step [396]
10.2b The finished product [401]
10.3 Propagation of imprecision [405]
10.4 Installing and customizing a macro [410]
10.4a  Installing external macros [410]
10.4b Assigning a shortcut key [411]
10.4c  Embedding in a menu [412]
10.4d Miscellany [414]
10.5 Fourier transformation [415]
10.5a  Forward Fourier transformation [416]
10.5b Descriptive notes [420]
10.5c  A bidirectional Fourier transformation macro [421]
10.6 Convolution and deconvolution [426]
10.7 Weighted least squares [432]
10.7a  The algorithm [432]
10.7b Implementation [433]
10.8 More about Solver [442]
10.8a  Adding uncertainty estimates to Solver [442]
10.8b Incorporating Solver into your macro [448]
10.9 Smoothing and differentiating equidistant data [449]
10.10 Semi-integration and semi-differentiation [460]
10.11 Reducing data density [463]
10.12 An overview of VBA [466]
10.12a  Objects [467]
10.12b  Properties and methods [467]
10.12c  Data types [468]
10.12d  Expressions [469]
10.12e  Statements [470]
10.12f  Active regions [470]
10.12g  Cells [471]
10.12h  Ranges [472]
10.12i  Subroutines [473]
10.12j  Macros [474]
10.12k  Functions [474]
10.12l  Message boxes [475]
10.12m Input boxes [475]
10.12n  Dialog boxes [476]
10.12o  Collective statements [476]
10.12p  For…Next loops [477]
10.12q  Do loops [478]
Contents
ix
10.12r  Conditional statements [479]
10.12s  Exit statements [480]
10.13 Summary [481]
Index [484]
x
Contents
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